【JIS日本標(biāo)準(zhǔn)】JIS Z 8462-3：2006 Capability of detection -- Part 3：Methodology for determination of the critical value for the response variable when no cal

z 8462-32005 (iso 11843-32003) 12 1 (jsa) iso 11843-3:2003capability of detection part 3: methodology for determination of the critical value for the response variable when no calibration data are used jis z 8462-3 a bjis z 8462 jis z 8462-1 1 jis z 8462-2 2 jis z 8462-3 3 1z 8462-32005 (iso 11843-32003) 11. 22. 23. 34. 34.1 34.2 34.3 35. yc 45.1 45.2 55.3 6 a 7 b8jisz 8462-32005(iso 11843-32003) 3 capability of detectionpart 3 : methodology for determination of the critical value for the response variable when no calibration data are used 2003 1 iso 11843-3:2003capability of detectionpart 3: methodology for determination of the critical value for the response variable when no calibration data are used jis q 0030 jis z 8461 2z 8462-32005 (iso 11843-32003)1. 5.1 jis z 8462-2 iso/iec guide 21 idtmodneqiso 11843-3:2003capability of detectionpart 3: methodology for determination of the critical value for the response variable when no calibration data are used (idt)2. jis q 0030 iso guide 30terms and definitions used in connection with reference materials jis z 8101-1 1 iso 3534-1statisticsvocabulary and symbolspart 1 : probability and general statistical termsjis z 8101-2 2 iso 3534-2statisticsvocabulary and symbolspart 2: statistical quality control jis z 8101-3 3 iso/fdis 3534-3statisticsvocabulary and symbolspart 3: design of experiments jis z 8402-2:1999 2 iso 5725-2:1994accuracy (trueness and precision) of measurement methods and resultspart 2:basic method for the determination of repeatability and reproducibility of a standard measurement method jis z 8461:20013z 8462-32005 (iso 11843-32003) iso 11095:1996linear calibration using reference materials jis z 8462-1:2001 1 iso 11843-1:1997capability of detectionpart 1: terms and definitions jis z 8462-2:2003 2 iso 11843-2:2000capability of detectionpart 2: methodology in the linear calibration case iso 5479:1997statistical interpretation of datatests for departure from the normal distribution3. jis z 8101jis q 0030jis z 8402-2jis z 8461jis z 8462-1 iso 5479 4.4.1 4.2 jis z 8462-2 4.1 4.34.3.1j j 30 95 30 4z 8462-32005 (iso 11843-32003) s5.2 sb 1 s s s vs221 (v ) yc | x = 0) (1)p( ya yc | x = 0) x = 0 ya yc 5z 8462-32005 (iso 11843-32003) 3 a)y 0 b)c)(1)(2)yc = yb z1 01 + 1j k (2)z1- 1 0jyb k 0 v s0 z1- t y = y t(v)s1 + 1 (3)cb10 jk (2)0b b sb 0 5.2 iso 5479 j y b =j y jj =1j y y y0 sb =j ( y j yb ) 2j =1j 1 y b 6z 8462-32005 (iso 11843-32003)y = y t(v)s1 + 1 (4)cb1b jk v = j 1 jis z 8462-1 0.05 t (2)(5) 1 yc = yb t1(v)sb1 + 1 (5)j (2)5.3 j sb k 0.05 1 1 jk (0.05) ybyasbyc k 7z 8462-32005 (iso 11843-32003) ab2j j = 12j kpssst t w=xyybyaycyj yoz 1 1 = j 1t 2 0b 28z 8462-32005 (iso 11843-32003) bb.1 1 icp-aes bcr bcr: community bureau of reference european commission (belgium) crm 142 bcr crm 142 light sandy soil0.5 g 10 1 25 ml 24 icp-aes 226 nm j30 b.1 crm 142 226 nm mv2.1702.2112.2062.2292.2152.2102.1912.1892.2152.1862.1832.1892.1452.1592.2092.1692.1942.1882.2032.1922.1912.2032.1752.2032.1742.1932.1712.1822.1782.172= 29 = 0.05 t t1-() = t0.95(29) =1.699 yb =2.189 8 mv sb = 0.018 6 mv 3 2.177 mv2.183 mv2.161 mv(4) 3 3 11yc =2.189 8+1.6990.018 6 =2.189 8+0.019 1 mv=2.209 mv b.2 +mv3039z 8462-32005 (iso 11843-32003) b.2 crm 142 226 nm yc3030.052.189 8 mv2.173 7 mv0.0186 mv2.209 mv (0.815 mv) 0.027 mv iacr b.2 2 (iii) cod jis jis k 0102 3 17.19.20.20 (codcr) (iii) (ii)30 0.060 mol/l (iii) b.3 b.3 ml19.7719.7119.7719.9419.9219.8419.7719.7119.7719.9119.9519.8819.7819.7119.8519.9419.9419.7719.7819.8019.8519.9119.9419.7619.7619.8319.7819.9119.8319.80= = 0.01 b2 = 1.737 1.79 5.12= = 0.05 w = 0.904 5 =10z 8462-32005 (iso 11843-32003)0.01 0.900= 0.05 0.927 1 yb = 19.829 ml sb = 0.0