中藥學(xué)專業(yè)論文.doc

湖南中醫(yī)藥大學(xué)畢業(yè)論文胃康靈膠囊質(zhì)量標(biāo)準(zhǔn)研究專業(yè)：中藥學(xué)目錄中文摘要1英文摘要21實(shí)驗(yàn)材料31.1藥品與對(duì)照品31.2儀器與試劑32薄層鑒別32.1甘草的薄層鑒別32.2白及的薄層鑒別42.3延胡索的薄層鑒別42.4三七的薄層鑒別53質(zhì)量標(biāo)準(zhǔn)研究63.1色譜條件的選擇63.2標(biāo)準(zhǔn)曲線的繪制與線性范圍考察83.3供試品溶液的制備93.4陰性對(duì)照實(shí)驗(yàn)103.5穩(wěn)定性實(shí)驗(yàn)123.6重現(xiàn)性試驗(yàn)123.7加樣回收率試驗(yàn)134樣品測(cè)定135結(jié)果與討論14參考文獻(xiàn)15致謝161中文摘要目的：研究并確定胃康靈膠囊的質(zhì)量標(biāo)準(zhǔn).方法:采用TLC法及HPLC法對(duì)胃康靈膠囊進(jìn)行鑒別和含量檢測(cè),采用DiamonsilC18色譜柱:以乙腈-0.1%磷酸溶液(14:88)為流動(dòng)相:流速:1.0ml/min:柱溫:30:檢測(cè)波長(zhǎng)為230nm結(jié)果:按改進(jìn)后的方法進(jìn)行實(shí)驗(yàn)，雜質(zhì)峰干擾較少，芍藥苷分離度及拖尾因子較好，而且大大縮短了進(jìn)樣測(cè)試時(shí)間。同時(shí)在TLC鑒別中排除了陰性是否有干擾.結(jié)論:TCL鑒別中陰性無(wú)干擾，含量測(cè)定改進(jìn)方法后實(shí)驗(yàn)較滿意，可以確定為其質(zhì)量標(biāo)準(zhǔn)關(guān)鍵詞：質(zhì)量標(biāo)準(zhǔn)；薄層鑒別；高效液相2ABSTRACTObjective:TostudyanddetermineWeikanglingcapsulesqualitystandards.Methods:TLCmethodandHPLCmethodwereusedforidentificationandtestingofWeikanglingcapsule,usingDiamonsilC18column,acetonitrile-0.1%phosphoricacid(14:88)ataflowrate:1.0ml/min,temperature:30,detectionat230nm.Results:byimprovedofthemethodofexperiment,lessinterference-impurities,paeoniflorinisolationandtailingfactorBetter,butalsoshortenedthesampletestingtime.andthereisnointerferenceintheTLCidentification.Conclusion:TCLexperientshavenonegativeinterferenceintheidentification,determinationofimprovingthemethodsofmoresatisfactory,sowecantodetermin