材料現(xiàn)代研究方法(05物相分析)

1、X射線物相分析射線物相分析 102030405060708090100 0 5000 10000 15000 20000 25000 Intensity(cps.) 2Theta(deg) 1 2 3 4 5 6 7 8 9 10 X射線粉末衍射成像 應(yīng)用舉例 20406080100120140160 Intensity 2theta 應(yīng)用舉例應(yīng)用舉例 序號序號2 sinsin2 2 d (A)I/I0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 38.05 43.28 44.28 50.40 64.38 74.09 77.34 81.45 90.86 95.10

2、97.80 110.45 114.90 134.85 136.82 2.3649 2.0905 2.0456 1.8106 1.4459 1.2786 1.2328 1.1806 1.0813 1.0439 1.0222 0.9378 0.9138 0.8342 0.8284 100 80 31 28 18 11 16 6 9 3 1 7 6 6 5 應(yīng)用舉例應(yīng)用舉例 序號序號2 d (A)I/I0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 38.05 43.28 44.28 50.40 64.38 74.09 77.34 81.45 90.86 95.10 97

3、.80 110.45 114.90 134.85 136.82 2.3649 2.0905 2.0456 1.8106 1.4459 1.2786 1.2328 1.1806 1.0813 1.0439 1.0222 0.9378 0.9138 0.8342 0.8284 100 80 31 28 18 11 16 6 9 3 1 7 6 6 5 d (A)I/I0d (A)I/I0 2.359 2.044 1.445 1.231 1.1796 1.0215 0.9375 0.9137 0.8341 100 40 25 26 12 4 15 12 13 2.355 2.039 1.442 1.230 1.1774 1.0196 0.9358 0.9120 0.8325 100 52 32 36 12 6 23 22 23 試驗數(shù)據(jù)試驗數(shù)據(jù)40783Ag40784Au 應(yīng)用舉例應(yīng)用舉例 序號序號2 d (A)I/I0 2 4 6 9 10 15 43.28 50.40 74.09 90.86 95.10 136.82 2.0905 1.8106 1.2786 1.0813 1.0439 0.8284 80 28 11 9 3 5 試驗數(shù)據(jù)試驗數(shù)據(jù) 規(guī)一化 100 35 14 11 4 6 d (A)I/I0 2.088 1.808 1.278 1.09