康塔氮吸附數(shù)據(jù)處理

1、氮吸附數(shù)據(jù)處理一比表面分析（找出微孔分析最佳的5個點）方法：1打開軟件-打開數(shù)據(jù)（file-open）am3000010002000300040005000600070008000Autosorb1-Isother*JIAHGHOHGBO-DANJING120121204-1.ravFilegditSearchRataReduetionAnalysisMenuOperationsWindowHelp曲昶IV昌二Il|UseAlt-MorrightmousebuttonforfloatingmenuRelativePressure,P/Po2找點（最佳適合微孔分析的5個點）鼠標右鍵-選擇如下aA

2、00001000200030004000500060007000S000口回岡Autosorb1-Isother*JIAHGHONGBO-DAHJING120121204-1.ravUseAlt-Morlightmousebuttonforfloatingmenu卿Autosorb1-Is.f電腦如何截屏？圏FileEditSearchDataReductionAnalysisMenuOperationsWindowHelpH|J剖豳|(zhì)Jj0433(1L55T2RelativePressure,P/Pographic2PlotsatularDataFrintAllPrintReportsGen

3、erateReportFilEditAri：alys.isInformationEditReportSelectianRataReductionFarametE卜然后會出現(xiàn)如下的界面面是試選，0.3以內(nèi)的點先全選（微孔分析主要選0.3以內(nèi)的點，下同）勾上“M”Autosorb1IsotherBJIAMGHONGBO-DAHJING120121204-1.rawFileEditSearchDataReductionAnalyeieMenuOperationsWindowHelp普|楓3|剖豳|(zhì)蚩|0532113.EI230.02251.620A0.06172.072A0.08702.286A0.

4、11212.488A0.13702.679A0.16202.867A0.18703.049A0.21203.225A0.23703.395A0.26203.585A0.28673.896A0.31194.101AOKCancel?Help點setselected點OK3找線，觀察哪5個點是最佳選擇的點鼠標右鍵-點下圖所示的地方出現(xiàn)這個界面時，請觀察這些紅點，找出5個點幾乎是在一條線上的點Autosorb1TmnTaA二一丄d、ad)!、一0.0000.000033一46428.84819.2329-160.03S00.07000.10500.14000.17500.2100RelativePr

5、essure,P/Po口同岡UseAlt-MorrightmousebuttonforfloatingmenuAutosorb1電腦如何截屏？麼氮吸附數(shù)據(jù)處理.d.通過觀察，大概是0.28以內(nèi)的5個點在一條線上4精確選點點擊后。oo先取消剛剛的點全選剛剛的點找到“M”，選OFF點setselected選剛剛我們找好的那5個點，0.28以內(nèi)的5個（注意M的選項）點setselected5找出樣品的比表面數(shù)據(jù)點擊下圖位置Distributioaoo100020003000400050000007oao8000】簡圃graphic三FlotmI：Autosorb10:28TabulaDataAuto

6、sorb1-Isother*JIAHGHONGBO-DAHJING120121204-1.ravFileEditSearchData.Reduction.AnalyeieMenuOperationsWindowHelp直Ijjl剖豳|(zhì)Jj04444157551電腦如何截屏？曹氮吸酣數(shù)據(jù)處理.d.UseAlt-MorrightmousebuttonforfloatingmenuRelativePcessuce,P/PoEditEditDataMethodMethodMethodMethodMethodMultipointBETMicroporeMiciopen-eArialysiArialymi

7、FrintAllPrintReportsGenerateReportFileLarigmuirAlpha-smethodTgtalFoieVolumeAverageFoieSizetMethodfilicroporeAnalysisBJHPoreSizeDistributionDHMFDRHKSFDAsArialj;sisSizeDisttiButionRawDataaridTagsAn：alys,isInformationFLegortSelectionFieduetion.FarameteisIUIsotheimSinglePointBETMicroporeIriterE.olationP

8、oreiAiea-Volunie_PoreSireSummaryDFT&Monte-CarloMethodFractalDimension.Mmthods在出現(xiàn)的界面就是比表面數(shù)據(jù)面我解析這個數(shù)據(jù)P/PoMULTIPOINTBETVDluir.ecc/gSTPS202e-015.396E+018701e-011200e-013702e-01S200e-013-04923.22543-39503-5850Area5.03SE+016-674E+017.321E+017.923E+011.307E+01m?g2.536E+02Intercept=1.294E+01CmrrelaticnCceffi

9、cient0.9999322.050E+01這是我們選的5個點的數(shù)據(jù)P/PcVolujr.ecc/gSTPl-5202e-012.85SS39SE+011.8701e-013-049203SE+012-1200e-013.2254S74E+0123702e-013.3950321E+012.S200e-013_5850923E+01面的是比表面數(shù)據(jù)Area1.307E+01m？代表m2/g,左邊的數(shù)據(jù)為13.07m2/g)面是我們所選擇的5個點的線性相關(guān)性C口rrelationCoefficient0-999932，這個數(shù)據(jù)沒有3個“9”以上不能用，得重新選點，要么就得重新測氮吸附。二孔徑，孔

10、體積分析相對比表面，這要簡單的多首先還是選點全選所有的點，剛剛選的5個點不用管SwitchOnOffSetSelectedICancel?HelpPressureVolumeFlags0.33804.299D0.31304.109D0.28803.908D0.26303.598D0.23813.403D0.21313.233D0.18803.056D0.16302.874D0.13812.687D0.11312.496D0.08802.294D-0.06312.084D0.03821.801D0.02611.661D2earAllIbSelectAll：|DeleteSelectedPoint

11、sI5.801.93E0.0000.00000.1000AdsorptionDesorptionMulti-PointBETSinglePointBETStatisticalThicknessPoreVolumeLangmuirDataPoreSizeDistributionDR.DAandFiactal0.20000.30000.40000.50000.60000.70000.80000.90001.0000RelativePressure,P/PoUseAlt-Morrightmousebuttonforfloatingmenu令開始Autosorb1-I:電腦如何截屏？勒氮吸附數(shù)據(jù)處理.

12、d.乜匚”)GQ10:39選擇上“p”點setselected找出后綴為“AD”的點，選擇上“V”Autosorb1-IsotherBJIAHGHOMGBO-DAKJIMG120121204-1.rarFileEditSearchDataReductionAnalyeieMenuOperationsWindowHelpffH|1g|Bl|?|麗弼15.2219EditRavDataandTagsUseAlt-Morrightmousebuttonforfloatingmenu0.78678.092APA0.81178.377AP0.83668.679AP0.85979.460AP0.88619

13、.986AP0.910910.586AP2l0.935311.433AP0.958912.748AP0.981115.027AP0.997418.431ADP0.973814.324DP0.943811.903DP0.915010.727DP0.888410.154DPV百開始Is.$電腦如何截屏？曹氮吸酣數(shù)據(jù)處理.d.10:42點setselected點ok即可完成所有選點。查看孔徑，孔體積Autosorb1-Isother*JIAHGH0KGB0-DAHJING120121204-1.rav口回岡IFileEditSearchData.Reduction.AnalyeieMenuOpera

14、tionsWindowHelp_oX聲M|J|昌豳?0.453314.9598O.IOOO0.20Q00.30000.40000.60000.70Q03.8711.935IsathennO.OQOO0.5000勺10:44UseAlt-MorrightmousebuttonforfloatingmenuAutosorb1-Is.電腦如何截屏？尊氮吸酣數(shù)據(jù)處理.d.出現(xiàn)的界面中如下：307E+01770H+01onAnalysis(BnLI一a;mnTa/lL2/11/2012UseAlt-Morlightmousebuttonforfloatingmenu)”豳Autosorb1$電腦如何截屏

15、|曹氮吸附數(shù)據(jù)處理-d.SO10:45AREA-VOLUME-FO&SSIZESUMMARYSUSFACEAHEADATAMultipointBETBJHMethodCuir.ulstiveAdsorptionSurfaceAreaBJHMethod.Cuir.ulstiveDesorptionSurfaceAreaHMethodCujt.u1stiveAdscrpticnSurfaceArea,DHMeth口dlCuir.ulstiveDescrpticnSurfaceArea1.307E+01m?g1.770E+01m?g1.792E+011.791E+01m?g1.B14E+01m?gF

16、OREVOLUMEDATATotalP口Volujr.e三口i:p口reswithRadiuslessthan3643.0?atP/Po=0.997392.833E-02cc/gBJHMethodCuir.ulstiveAdscrpticn片口EmVolujr.eBJHMethodCuir.ulstiveDesorptionF口eeVolujr.e3.043E-02cc/g3.0S1E-02cc/gHMethcdCujt.u1stiveHMethcdCujt.u1stiveAdsorptionPereVoluir.eDesorptionP口Voluir.e2.990E-02cc/g2.999E

17、-02cc/gAveracrePoreRadiu.34-337E+01BJHMethodAds口izptiGnPcreRadius(Mode)1.21BE+01二BJHMethcdDbs口zzpticnPcreRadius(Mode)1.221E+01二DHMethodAds口i:ptic：iiFereRadiusMode)1.21SE+01二DHMethcdDes口FereRadiusMode)1.221E+01IPORESIZEDATAATA&EDUCTTONEARAMETE&SThenr.alTranspiration:OFFLast;PoAcquired512-00itjt.HgMax

18、iDose:ONInitialFill:OFFD口seWizard:OFF第一組為比表面，第二組為孔體積，第三組為孔徑。每組都有5排數(shù)據(jù)，均要第一排數(shù)據(jù)，后面4排是不同的分析方法做得到的數(shù)據(jù)。先看比表面數(shù)據(jù)SUSFACE盤迄盤DATAMultipointBETBJH時ethedCuir.ulativeAdsorptionSurfa.ceAreaBJH時ethedCuir.ulativeDesorptionSurfa.ceAreaHMethcdCwr.ulativeAdsorptionSurfaceAres.HMethcdCwr.ulativeDesorpticnSurfaceAres.1.307E+-01m?g1.770E+-01m?g1.792E+-01m?g1.791E+-01m?g1.B14E+-01m?g比表面為13.07m2/g再看孔體積POEIETOLUMZDATATotalE口Volwr.eforporeswithRadius.S33E-02cc/g3.043E-02cc/g3.051E-02cc/g2.990E-02cc/g2.999E-02cc/glessthan3643.0?atP/Pq=0.99739BJHMethodCuir.ulsti