油基鉆井液用有機(jī)土 編制說明

《油基鉆井液用有機(jī)土》編制說明 1 4.編制原則、相關(guān)標(biāo)準(zhǔn)情況、標(biāo)準(zhǔn)檢驗(yàn) 1本標(biāo)準(zhǔn)來源于2023年第四批推薦性國家標(biāo)由TC355（全國石油天然氣標(biāo)準(zhǔn)化技術(shù)委員會(huì)）歸口，越來越高，對(duì)油基鉆井液處理劑的質(zhì)量和有效遴選著我國環(huán)保法律法規(guī)的要求日益提高，評(píng)價(jià)有機(jī)土用低于柴油中的含量，因此在白油中有機(jī)土更不易23.起草工作簡要過程有限公司勘探開發(fā)研究院、中國石油集團(tuán)工程技術(shù)研究院），3過程中要求樣品為25kg袋裝，降低了針對(duì)性送樣影4.編制原則、相關(guān)標(biāo)準(zhǔn)情況、標(biāo)準(zhǔn)檢驗(yàn)項(xiàng)目的確定各項(xiàng)檢測實(shí)驗(yàn)操作簡單可行，便于各油田實(shí)驗(yàn)室開的牌號(hào)為W1-110的白油。W1-110餾程、黏度區(qū)間窄，組分相對(duì)簡單，有利于取得穩(wěn)定的實(shí)驗(yàn)評(píng)價(jià)數(shù)據(jù)，同時(shí)，W1-110在中石油、中海油均有較為廣泛的應(yīng)用，綜合上述），4Q/SY17817-2021針對(duì)油基鉆井液用有機(jī)土，制訂了相應(yīng)的理化井液用有機(jī)土PF-MOGEL制訂了相應(yīng)的理化性能技針對(duì)油基鉆井液用有機(jī)土，制訂了基于低溫（3其他民營企業(yè)的企業(yè)標(biāo)準(zhǔn)則參差不齊?？偟膩碚f，中石油和中石化產(chǎn)品標(biāo)準(zhǔn)相對(duì)接近，可達(dá)到同等的提切效果，浪費(fèi)了大量成本；另一方面，由于低質(zhì)有機(jī)土的使用和累積，1有機(jī)膨潤土52油基鉆井液用有機(jī)土技術(shù)規(guī)范Q/SY17817-20213油基鉆井液用有機(jī)土技術(shù)要求Q/SHCG0190-2023（中石化）4鉆井液用有機(jī)土PF-MOGELQ/HSYFOC027—20215油基鉆井液用有機(jī)土Q/ZFH03-20216油基鉆井液用增粘劑有機(jī)土PLH-OCQ/12DGPLH02-20177油基鉆井液用有機(jī)土Q/0305ZLJ001-20188油基鉆井液用增粘劑改性有機(jī)土HFISQ/74961404-7.66-20179油基鉆井液用增粘劑改性有機(jī)土ZR-02Q/91510681777452735M.35-2018油基鉆井液用增粘劑有機(jī)土TYODF-601Q/KTYC049-2018油基鉆井液用提粘劑有機(jī)土LH-OCQ/LHSY0028-2017油基鉆井液造漿用有機(jī)膨潤土CNLQ/915108246922987249-2017油基鉆井液用有機(jī)膨潤土Q/SH1170053-2017油基鉆井液用提粘劑改性有機(jī)土HYOTQ/WNZJ-034-2018油基鉆井液用有機(jī)土ZD-JHAQ/ZDSY008-2017白油基鉆井液用有機(jī)土Q/GWDC0073-2017油基鉆井液用增粘劑有機(jī)土TYODF-601Q/KTYC049-2018油基鉆井液用提切劑有機(jī)土BZ-OCQ/12SYBHZ1002-2016油基鉆井液用有機(jī)土MOGELQ/JHK1018-2018油基鉆井液用提粘劑改性有機(jī)土(HYOT)Q/WNZJ-034-2015油基鉆井液用有機(jī)土活化蒙脫石JX-GELQ/KJX12-2019油基鉆井液造漿用有機(jī)土（HFEL）Q/74961404-7.55-2014有機(jī)土MOGELQ/JJH26-2015鉆井液用有機(jī)土改性膨潤土ATOQ/KOZ-013-2018油基鉆井液用增粘劑有機(jī)土TYODF-601Q/KTYC049-2016編號(hào)標(biāo)準(zhǔn)名稱評(píng)價(jià)項(xiàng)目技術(shù)要求1Q/SHCG0190-2023（中石化）外觀灰白色或淺黃色粉末水分，%≤4.0篩余量（篩孔孔徑74μm），%≤4.0灼燒失量，%27.0~40.06編號(hào)標(biāo)準(zhǔn)名稱評(píng)價(jià)項(xiàng)目技術(shù)要求），70.0/室溫120℃老化16h表觀黏度，mPa·s≥動(dòng)切力，Pa≥2.03.0動(dòng)塑比，Pa/mPa·s≥0.300.30R3讀值≥2.03.0API濾失量，mL≤8.08.0*注：白油基有機(jī)土采用5號(hào)白油作為基礎(chǔ)油進(jìn)行測試2Q/SY17817-2021（中石外觀灰白色或淺黃色粉末烘失量，%≤4.0篩余量0.074mm（200目），%≤4.0灼燒殘?jiān)?58.0～70.0堆積密度，g/cm30.40～0.55≥70.0/熱滾前120℃熱滾后3r/min讀值≥2.0≥3.0動(dòng)切力，Pa≥2.0≥3.0動(dòng)塑比，Pa/(mPa·s)≥0.30≥0.30濾失量，mL≤8.0≤8.0白油基有機(jī)土采用5號(hào)白油，柴油基有機(jī)土采用0號(hào)柴油3Q/HSYFOC027-2021（中海油）外觀灰白或白色自由流動(dòng)粉末水分，%≤5細(xì)度（100目），%≥95塑性粘度（120℃老化后），mPa·s≤13動(dòng)切力（120℃老化后），Pa≥36轉(zhuǎn)讀數(shù)（120℃老化后）≥44Q/ZFH03-2021（浙江豐外觀自由流動(dòng)固體粉末水份，%≤5.0≤5.0/柴油基有機(jī)土有機(jī)土膠體率（span80），%≥95.0≥95.0表觀粘度，mPa·s≥8.0≥8.0動(dòng)切力，Pa≥1.5≥1.5R3讀數(shù)≥1.5≥1.5序號(hào)外觀水分篩余膠體率表觀粘度，mPa.塑性黏度，mPa.動(dòng)切力，Pa6r/min穩(wěn)定性,濾失量，mL灼燒失重動(dòng)切力提動(dòng)塑比7ssV高率數(shù)量21614312占比70.83%87.50%75.00%66.67%54.17%54.17%62.50%25.00%4.17%%%4.17%8.33%（74μm）標(biāo)準(zhǔn)篩測試試樣的篩余量，有利于有機(jī)土利用要用到大量水，為考核產(chǎn)品有效成分含量，擬設(shè)置烘8）；m1——烘前試樣質(zhì)量加稱量瓶質(zhì)量，單位）；9樣品編號(hào)105℃烘失量，%170℃烘失量，%①②平均值平行允差①②平均值平行允差2.742.952.80.217.136.496.80.642#3.032.792.90.246.276.356.30.083#2.732.732.707.297.757.50.464#0.237.217.207.20.015#2.312.482.40.176.155.960.196#2.903.300.408.207.607.90.607#3.464.013.70.557.847.50.730.457.727.757.70.039#3.343.523.40.187.577.597.60.023.683.613.60.077.007.767.40.763.133.763.40.637.297.257.30.042.923.290.376.316.486.40.173.723.673.70.056.345.996.20.353.783.713.70.077.007.187.10.182.492.822.70.337.617.677.60.062.252.392.36.195.505.80.692.302.272.30.036.676.906.80.230.285.706.316.00.613.663.613.60.056.796.816.80.0220#4.244.274.30.03————21#4.254.284.30.03————22#4.304.314.30.01 23#2.972.922.90.05 24#5.425.555.50.13————25#4.043.874.00.17————26#0.01 ①②123456789此以此以74μm標(biāo)準(zhǔn)篩測試試樣的篩余量。擬定以下實(shí)驗(yàn)方法：不再有試樣通過時(shí)為止，將標(biāo)準(zhǔn)篩上部的試樣倒出X——篩余量；）；樣品編號(hào)篩余量，%①②平均值平行允差2#0.020.030.00.013#0.880.940.90.064#0.640.540.60.105#2.162.10.046#2.312.482.40.177#3.583.343.50.242.542.502.50.049#0.012.742.622.72.922.882.90.043.643.753.72.822.802.80.020.130.040.440.420.40.022.732.752.70.022.912.882.90.033.003.063.00.0620#3.984.044.00.0621#4.284.204.20.0822#5.265.185.20.0823#2.702.792.70.0924#4.644.754.725#2.882.752.80.1326#4.784.824.80.04樣品編號(hào)篩余量，%①②平均值12.532.512.52樣品編號(hào)篩余量，%①②平均值23.233.223.23342.522.482.5053.603.583.59672.502.462.4882.202.232.2292.542.522.534.804.754.783.152.312.482.403.583.343.462.542.502.522.742.622.682.922.882.903.643.753.702.822.802.81203））；m6——灼燒后瓷坩堝加殘?jiān)馁|(zhì)量，單位可知：1）700℃灼燒，75%樣品灼燒殘?jiān)橛?0根據(jù)試驗(yàn)數(shù)據(jù)得出，700℃和900℃兩個(gè)溫度下，灼燒殘?jiān)慕Y(jié)果變確定灼燒殘?jiān)臏囟葹?00℃。對(duì)收集到的26個(gè)樣品在樣品編號(hào)灼燒失量，%①②平均值平行允差39.2739.3339.30.062#40.7340.740.70.033#33.9634.1344#36.1936.3936.30.25#38.3138.4138.40.16#33.0733.0933.10.027#33.7733.7533.80.0238.1337.94380.199#33.233.1733.20.0332.7732.8132.80.0433.9634.13340.1733.5333.4733.50.0629.629.6329.60.0329.4629.5129.50.0538.4638.5738.537.437.3537.40.0537.6437.6337.60.0135.5235.5735.50.0536.2736.2636.30.0120#33.1733.1833.20.0121#34.9435.9735.522#32.6332.8132.70.1823#29.6330.4300.7724#37.3337.5437.40.2125#39.7740.22400.4526#35.3735.3935.40.02編號(hào)灼燒失量，%①②平均值138.6138.6238.62231.0131.0331.04332.0332.08439.4039.3539.38531.7131.7931.75629.6229.6429.63732.1932.2432.22835.0535.0535.05930.3230.4030.3628.3228.2228.2732.6032.6532.62密度樣品編號(hào)有機(jī)土在5#白油中膠體率，%有機(jī)土在0#柴油中膠體率，%50℃65℃120℃150℃50℃65℃120℃150℃175939998240699565979596953262730314303136375719598989868.4—909292—78.29 69 82827.531—929892.5—98.59.57—91.547.5—8—9492.5—232228—9077—58298—90—724359—90 71 586058—356—373256—40464545737894—20252934—253936—202428242421222730332288823232124212528289393939025314058382636353642V——90min時(shí)量筒上部析出的游離油體積，單位為毫升（m表13有機(jī)土樣品膠體率初步測試（號(hào)四川0號(hào)柴油1234567895②采用北京、四川、山東不同地域市售0號(hào)柴油進(jìn)行的膠體率實(shí)驗(yàn)數(shù)據(jù)分析，在室率同比四川高25%~64%；120℃老化后，表現(xiàn)出同樣的膠體率規(guī)律，表明不同地域間0采用北京市售0號(hào)柴油膠體率≥85%樣品有2種，占采用四川德陽市售0號(hào)柴油膠體率≥85%樣品 采用山東德州市售0號(hào)柴油膠體率≥85%樣品有③在中海油服實(shí)驗(yàn)室，取8#和11#有機(jī)土樣品，采用不同地域的柴油在中海油服實(shí)%驗(yàn)。中石油工程院實(shí)驗(yàn)中，有4個(gè)樣品升溫至150℃后，膠體率上升，1個(gè)樣品升溫后降降低地域間柴油油品質(zhì)量對(duì)膠體率的影響，膠體率≥70%作為膠體率指標(biāo)，白油基有機(jī)土膠體率≥編號(hào)膠體率（%）120℃150℃180℃1959429290753384935426377874883346589643834209090編號(hào)膠體率%120℃150℃180℃192942949075345716556558779727086570689443224333025757970編號(hào)膠體率%120℃150℃180℃199999927578374493570756564569577777487953931285850457073性明顯低于柴油，有機(jī)土在白油中膠體率較低編號(hào)膠體率（%）常溫120℃150℃180℃1282823238492225235667768897597表193#白油老化后膠體率（編號(hào)膠體率（%）120℃150℃180℃1232128342123215697898788編號(hào)膠體率%120℃150℃180℃12129739994599967877888898875549在柴油中加入0.5%乙醇，測試室溫下流變），中6.3方法測定基漿和試驗(yàn)漿在25℃±1℃下動(dòng)切力、動(dòng)塑比和Φ3讀值。樣品編號(hào)5#白油老化條件φ600φ300AVPVYP，PaYp/PV,Pa/mPa.sφ3HTHP,mL0#25.50.70.060-常溫25.50.70.060全濾150℃/16h794639.5336.50.206-常溫6757470.216.538150℃/16h2#664333230.437-常溫樣品編號(hào)5#白油老化條件φ600φ300AVPVYP，PaYp/PV,Pa/mPa.sφ3HTHP,mL412220.50.08156150℃/16h5#714235.5296.50.224.5-常溫985949390.266.036150℃/16h97.55443.50.8147-常溫276500.5766太稠，無濾液150℃/16h76.548.538.2280.379.0-常溫90.550.045.240.54.83.062150℃/16h936741260.6323-常溫>300231////52.0150℃/16h樣品編號(hào)0#柴油老化條件φ600φ300AVPVYP，PaYp/PV,Pa/mPa.sφ3HTHP,mL0#65410.250-常溫5.554.50.50.5全濾150℃/412620.55.50.375-常溫654132.5248.50.35735150℃/2#35245.50.506-常溫86.550.300.274150℃/5#362240.295-常溫5635282170.33539150℃/7#83.560.541.8230.7826-常溫22521097.56.2424150℃/52352690.518-常溫樣品編號(hào)0#柴油老化條件φ600φ300AVPVYP，PaYp/PV,Pa/mPa.sφ3HTHP,mL6144270.6024150℃/9#7454.5370.8620-常溫7232.539.56436150℃/91.565.545.8260.7623-常溫>300236////9820150℃/614430.50.85-常溫90664524210.8832150℃/77.053.538.523.50.64-常溫71.537.034.50.9371.026.0150℃/48.530.024.25.80.315.5-常溫74.051.529.022.50.7826.033.6150℃/老化和滾動(dòng)老化條件，分別測流變性和中壓濾失量；②120℃/），加樣量Φ600Φ300Φ3AVPVYPYP/PVAPIFL,mL2%0.58.570.2143%24.529.52.750.293.44%42.529821.257.750.575%532441290.413.2加樣量Φ600Φ300Φ3AVPVYPYP/PVAPIFL,mL2%9187143%2320.152.34%34213.540.3135%654632.50.712.1加樣量Φ600Φ300Φ3AVPVYPYP/PVAPIFL,mL2%9.5186.50.232.33%21282.50.314%35234.55.50.465%644432200.6加樣量Φ600Φ300Φ3AVPVYPYP/PVmL2%9.5186.50.23223%25393.50.392104%4932824.57.50.445%7854.53923.50.66b）柴油中有機(jī)土加量測試實(shí)驗(yàn)化和滾動(dòng)老化條件，分別測流變性和中壓濾失量；②120℃/16加樣量Φ600Φ300Φ3AVPVYPYP/PVAPI2%86420.54.63%203730.434.24%372687.50.684.45%624821314.1加樣量Φ600Φ300Φ3AVPVYPYP/PVAPI2%75.540.385.53%2.58620.334.74%33237.56.50.654.55%564333283.8加樣量Φ600Φ300Φ3AVPVYPYP/PVAPI2%6.515.2540.315.93%38530.65.24%3322.5760.575.05%503820255.2加樣量Φ600Φ300Φ3AVPVYPYP/PVHTHP2%86.550.303%2247.53.50.474%5036250.795%66494224208滾后的性能測試條件為65℃±1℃。滾16h前后的65℃下的流變性和中壓濾失量，實(shí)驗(yàn)3測試溫度65℃±1℃34試溫度度65℃±1℃385測試溫度65℃±1℃55試溫度度65℃±1℃2測試溫度65℃±1℃試溫度度65℃±1℃9測試溫度65℃±1℃98試溫度度65℃±1℃764測試溫度65℃±1℃9試溫度度65℃±1℃4測試溫度65℃±1℃77試溫度度65℃±1℃86420987動(dòng)切力，Pa動(dòng)切力，Pa5432100.40.30.20.10.0中壓濾失量，mL中壓濾失量，mL543210mm熱滾前量樣品編號(hào)φ600φ300φ3AVPVYPPaYp/PVPa/mPa.sFL,mL實(shí)驗(yàn)條件29.572.50.364.7測試溫度65℃±1℃2237.53.50.475.7試溫度度65℃±1℃2#2.57.254.52.750.613.5測試溫度65℃±1℃24.54.57.54.750.635.6試溫度度65℃±1℃5#8.7570.254.4測試溫度65℃±1℃2.59.7572.750.395.8試溫度度65℃±1℃7#3827880.734.4測試溫度65℃±1℃4028.5208.50.743.8試溫度度65℃±1℃234.574.50.644.5測試溫度65℃±1℃213.56.540.625.2試溫度度65℃±1℃9#422992180.625.5測試溫度65℃±1℃3625.59.57.50.716.5試溫度度樣品編號(hào)φ600φ300φ3AVPVYPPaYp/PVPa/mPa.sFL,mL實(shí)驗(yàn)條件65℃±1℃42292180.624.7測試溫度65℃±1℃47.53323.89.20.634.8試溫度度65℃±1℃30.5216.59.55.750.614.5測試溫度65℃±1℃31.5227.59.56.20.655.6試溫度度65℃±1℃2.57.7552.750.553.7測試溫度65℃±1℃3926.5670.567.7試溫度度65℃±1℃18.256.50.277.1測試溫度65℃±1℃730.53.54-0.5-全濾失試溫度度65℃±1℃24#213.574.50.645.2測試溫度65℃±1℃38.862.70.456.2試溫度度65℃±1℃φ3讀值86420圖18柴油中有機(jī)土熱滾前、后φ3讀值動(dòng)切力，Pa98765432100.70.60.50.40.30.20.10.01#2#5#7#8#9#10#12#17#24#中壓濾失量，mL876543210mm熱滾前1#2#5#7#8#9#10#12#17#24#量），項(xiàng)目技術(shù)要求白油基鉆井液用有機(jī)土柴油基鉆井液用有機(jī)土外觀灰白色或淺黃色粉末灰白色或淺黃色粉末烘失量，%≤4.0≤4.0篩余量，%≤4.0≤4.0灼燒殘?jiān)?58.0～70.058.0～70.0堆積密度，g/cm3≤0.55≤0.55膠體率，%≥70.0≥70.0室溫Φ3讀值≥2.0≥2.0動(dòng)切力，Pa≥2.0≥2.0動(dòng)塑比，Pa/mPa.s≥0.30≥0.30API濾失量，mL≤8.0≤8.0120℃熱滾Φ3讀值≥3.0≥3.0動(dòng)切力，Pa≥3.0≥3.0動(dòng)塑比，Pa/mPa.s≥0.30≥0.30API濾失量，mL≤8.0≤8.0注：流變性測試溫度65℃±1℃。將上述配制好的柴油膠體溶液，裝入高溫不銹鋼罐中，充氮?dú)庵?MPa，持續(xù)時(shí)間好分散及成膠能力，其他測試樣品在柴油中分散性較差，編號(hào)120℃老化R600R300R6R3AVPVYPPa動(dòng)塑比1老化前2255740.57老化后217.5764.50.752老化前73003.54//老化后73003.54//3老化前5005.0500.00老化后6105.0410.254老化前84004.0400.00編號(hào)120℃老化R600R300R6R3AVPVYPPa動(dòng)塑比老化后95004.540.50.135老化前95004.540.50.13老化后7005.540.386老化前63003.0300.00老化后63003.0300.007老化前74003.530.50.17老化后5105.0500.008老化前84004.0400.00老化后5005.0500.009老化前84004.0400.00老化后73003.54//老化前95004.540.50.13老化后6105.550.50.10老化前95004.540.50.13老化后5005.0500.00老化前215473.50.50老化后2076730.43老化前63003300.00老化后84004400.00老化前74003.530.50.17老化后5105500.00老化前74003.530.50.17老化后95104.540.50.13老化前73003.54-0.5-0.13老化后95004.540.50.13老化前73003.54-0.5-0.13老化后84004400.00老化前84004400.00老化后6105410.25老化前73003.54-0.5-0.13老化后95004.540.50.1320老化前95004.540.50.13老化后5105500.00編號(hào)120℃老R600R300R6R3AVPVYPPa動(dòng)塑比1老化前328620.33老化后559540.82老化前5005500老化后6105410.253老化前84004400編號(hào)120℃老R600R300R6R3AVPVYPPa動(dòng)塑比老化后95004.540.50.134老化前95004.540.50.13老化后7005.540.385老化前74003.530.50.17老化后51055006老化前73003.54--老化后73003.54--7老化前84004400老化后840044008老化前63003300老化后630033009老化前73003.54--老化后73003.54--老化前63003300老化后63003300老化前84004400老化后5005.0500老化前327.552.50.50老化后548.562.50.42老化前63003.0300.00老化后74003.530.50.17老化前74003.530.50.17老化后85104.0310.33老化前74003.530.50.17老化后95104.540.50.13老化前73003.54-0.5-0.13老化后95004.540.50.13老化前73003.54-0.5-0.13老化后84004.0400.00老化前84004.0400.00老化后6105.0410.25老化前73003.54-0.5-0.13老化后84004.0400.0020老化前84004.0400.00老化后95104.540.50.13AV=R600（5）PV=R600?R300（6）YP=R300?AV（7）Rdp=YP（8）R600——六速旋轉(zhuǎn)黏度計(jì)600r/min的讀數(shù)；R300——六速旋轉(zhuǎn)黏度計(jì)300r/min的讀數(shù)；YP——?jiǎng)忧辛?，單位為帕（Pa）；PV——塑性黏度，單位為毫帕秒（mPa?s）；測出數(shù)據(jù)。表明，采用不同煉化公司的柴油，有機(jī)土在其中的增粘提切效果有所區(qū)別，從實(shí)驗(yàn)數(shù)據(jù)看，在四川老化前后流變參數(shù)明）；根據(jù)實(shí)驗(yàn)分析，Span80作為乳化劑，抗溫作用有限，Span8表36柴油基鉆井液高溫流變性實(shí)驗(yàn)（編號(hào)老化R3AVPVYPPa動(dòng)塑比FLAPImL1老化前283.50.445.4120℃老化65.00.506.0150℃老化25.09.00.566.8180℃老化23.58.50.577.22老化前54.00.405.4120℃老化44.50.455.8150℃老化34.0200.707.4180℃老化動(dòng)3老化前2.594.00.446.4120℃老化34.00.405.8150℃老化927.50.628.0180℃老化動(dòng)4老化前395.50.616.0120℃老化34.00.40150℃老化27.59.50.53180℃老化動(dòng)5老化前294.00.445.8120℃老化55.00.507.2150℃老化26.50.668.2180℃老化30.0200.507.86老化前2.54.00.366.6120℃老化55.00.427.0編號(hào)老化R3AVPVYPPa動(dòng)塑比FLAPImL150℃老化2238.5260.489.2180℃老化動(dòng)7老化前55.50.462.4120℃老化822.58.50.615.8150℃老化33.5249.50.408.6180℃老化46.5310.509.48老化前295.00.564.4120℃老化65.00.455.4150℃老化22.08.00.577.8180℃老化27.50.628.69老化前584.50.565.2120℃老化86.50.546.8150℃老化43.5300.457.5180℃老化動(dòng)老化前273.00.437.2120℃老化34.00.406.6150℃老化21.07.00.50180℃老化動(dòng)老化前394.00.445.8120℃老化55.50.557.0150℃老化520.56.50.468.4180℃老化334.0230.48表37柴鉆井液高溫流變性實(shí)驗(yàn)（編號(hào)老化溫度Φ3AVPVYPPa動(dòng)塑比FLAPImL1老化前34.50.454.9120℃老化76.00.466.8150℃老化25.50.707.5180℃老化無法流動(dòng)2老化前44.00.364.0120℃老化25.50.707.2150℃老化25.08.02.138.3180℃老化無法流動(dòng)3老化前45.00.454.0120℃老化922.58.50.616.4150℃老化935.021.00.678.6180℃老化無法流動(dòng)4老化前820.55.50.37編號(hào)老化溫度Φ3AVPVYPPa動(dòng)塑比FLAPImL120℃老化30.50.61150℃老化28.50.68180℃老化無法流動(dòng)5老化前29.57.02.50.363.2120℃老化39.03.50.394.8150℃老化923.57.50.478.0180℃老化31.021.00.487.56老化前27.03.50.504.0120℃老化55.50.506.9150℃老化3341.026.00.588.6180℃老化無法流動(dòng)7老化前39.04.00.443.7120℃老化820.56.50.466.4150℃老化36.024.00.509.5180℃老化2050.535.00.448老化前58.05.50.694.9120℃老化26.521.05.50.267.0150℃老化26.00.637.6180℃老化26.00.639老化前43.50.324.0120℃老化25.00.676.6150℃老化2548.533.00.478.3180℃老化無法流動(dòng)老化前55.50.466.0120℃老化722.57.50.507.4150℃老化5544.024.020.00.839.6180℃老化無法流動(dòng)老化前33.50.355.2120℃老化55.00.367.0150℃老化35.024.00.468.2180℃老化無法流動(dòng)老化前17.56.00.25120℃老化49.05.00.566.6150℃老化29.00.179.4180℃老化0.59.08.00.13表38柴油基鉆井液高溫流變性實(shí)驗(yàn)（中石編號(hào)老化溫度Φ3AVPVYPPa動(dòng)塑比FLAPImL1老化前394.50.505.4120℃老化340.366150℃老化230.924.4編號(hào)老化溫度Φ3AVPVYPPa動(dòng)塑比FLAPImL180℃老化無法流動(dòng)2老化前43.50.327.2120℃老化280.756.8150℃老化無法流動(dòng)180℃老化無法流動(dòng)3老化前340.405.8120℃老化280.659.2150℃老化無法流動(dòng)180℃老化無法流動(dòng)4老化前550.505.4120℃老化26.50.6637150℃老化32200.6046180℃老化無法流動(dòng)5老化前2.5830.387.4120℃老化77.50.686.5150℃老化26.50.778.4180℃老化32.5200.639.26老化前3760.867120℃老化280.567150℃老化2036210.71180℃老化無法流動(dòng)7老化前2940.447.2120℃老化550.507.4150℃老化無法流動(dòng)180℃老化無法流動(dòng)8老化前44.50.456.8120℃老化270.937.2150℃老化290.718.3180℃老化32.50.919老化前560.506120℃老化290.819150℃老化無法流動(dòng)180℃老化無法流動(dòng)老化前29630.508.2120℃老化24.59.50.639150℃老化無法流動(dòng)180℃老化無法流動(dòng)老化前340.367120℃老化922.58.50.618150℃老化250.798.5180℃老化無法流動(dòng)120℃、150℃、180℃的流變性和濾失量。流變性與柴油基）；），），Φ3≥3（90%），API濾失量≤8mL（7表39白油基鉆井液高溫流變性實(shí)驗(yàn)（FLAPI278358動(dòng)35動(dòng)582445動(dòng)3動(dòng)3246動(dòng)FLAPI348動(dòng)25動(dòng)表40白油基鉆井液高溫流變性實(shí)驗(yàn)（編號(hào)老化溫度Φ3AVPVYPPa動(dòng)塑比FLAPImL老化前2930.336120℃老化55.50.509150℃老化290.71180℃老化434721262#老化前32.50.256120℃老化76.50.50150℃老化3335.5180℃老化無法流動(dòng)-3#老化前32.50.237120℃老化860.46150℃老化2335210.67180℃老化無法流動(dòng)-4#老化前660.469.2120℃老化92170.50150℃老化290.81180℃老化無法流動(dòng)5#老化前292.50.287.6120℃老化393.50.399.2150℃老化2170.50180℃老化無法流動(dòng)6#老化前392.50.2